The Techniques in NMR Spectroscopy

MEU INSTITUTE OF HEALTH SCIENCES COURSE SYLLABUS
Course title- course code: The Techniques
Programme name: Department of Analytical
in NMR Spectroscopy - (EAK 511)
Chemistry, Master of SCI Programme
MASTER OF SCI (Msc) X
Level
DOCTORATE
(PhD)
PREREQ. PREP.
Hours/week
Ther. Recite.Lab.
And cre dit
2
Language
-
-
Others Total
-
-
MEU Credit
2
ECTS Credit
2
Turkish
Compulsory /
Elective
Prerequisites Msc or PhD student
Course
Contents
Nuclear spin and resonance, The measurement of spectra, The chemical shift,
Factors affecting the chemical shift, Spin-spin coupling, Spin systems, Dynamic
NMR spectroscopy and The techniques in NMR spectroscopy; HETCOR, COSY
and NOE
Course
Objectives
Learning
Outcomes
and
Competences
Textbook
and /or
References
To explain the principle of NMR spectroscopy and the techniques in NMR
Complete to the criteria for to pass in the exams
Williams H. D., Fleming I. “Spectroscopic methods in organic chemistry”. Fourth
Edt. Revised, McGraw-Hill Book Company, England, 1989.
Balcı M. “Nükleer manyetik rezonans Spektroskopisi”. ODTU Gelistirme Vakfı
Yayıncılık ve Iletişim A.S. Firstly Ed. Ankara, 2000.
Skoog D.A., HollerF.J., Nieman T.A. “Enstrümantal Analiz Ilkeleri” Trans. Edit.
Kılıç E., Köseoğlu F., Yılmaz H. Fifth Ed. Saunders Golden Sunburst Series,
Philadephia, 1991.
Laboratory Work
Assessment
Crite ria
Other
Committee Exam
Instructors
Prof. Dr. H. Ali DONDAS
e-mail
[email protected]
X
100
Course Content
Week 1
Nuclear spin and resonance
Week 2
Nuclear spin and resonance
Week 3
The measurement of spectra
Week 4
The measurement of spectra
Week 5
The chemical shift
Week 6
The chemical shift
Week 7
Factors affecting the chemical shift
Week 8
Spin systems
Week 9
Spin-spin interaction
Week 10
Dynamic NMR spectroscopy
Week 11
The techniques in NMR spectroscopy HETCOR, COSY and NOE
Week 12
The techniques in NMR spectroscopy HETCOR, COSY and NOE
Week 13
Interpretation of NMR spectroscopy on the combined structure problems
Week 14
Interpretation of NMR spectroscopy on the combined structure problems